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AR Category: Laboratory Testing
Textile Abrasion Wear By Tribometer
The measurement of textile abrasion resistance of fabrics is very challenging. Many factors play a role during the test, including the mechanical properties of the fibers, the structure of the yarns and the weave of the fabrics. This may result in poor reproducibility of test results and create difficulty in comparing values reported from different laboratories. Wear performance of the fabrics is critical to the manufacturers, distributors, and retailers in the textile production chain. A well-controlled quantifiable and reproducible Tribometer wear resistance measurement is crucial to ensure reliable quality control of the fabric production.
Self Cleaning Glass Coating Friction Measurement
Self cleaning glass coating possesses a low surface energy that repels both water and oils. Such a coating creates an easy-clean and non-stick glass surface that protects it against grime, dirt and staining. The easy-clean coating substantially cuts the water and energy usage on glass cleaning. It does not require harsh and toxic chemical detergents, making it an eco-friendly choice for a wide variety of residential and commercial applications, such as mirrors, shower glasses, windows and windshields.
Cyclical Nanoindentation Stress-Strain Measurement
Cyclical Nanoindentation Stress-Strain Measurement
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Importance of Nanoindentation
Continuous stiffness measurements (CSM) obtained by nanoindentation reveals the stress-strain relationship of materials with minimally invasive methods. Unlike traditional tensile testing methods, nanoindentation provides stress-strain data at the nanoscale without the need of a large instrument. The stress-strain curve provides crucial information on the threshold between elastic and plastic behavior as the sample is subject to increasing loads. CSM gives the capability to determine the yield stress of a material without dangerous equipment.
Nanoindentation provides a reliable and user-friendly method to quickly investigate stress-strain data. Furthermore, measuring stress-strain behavior on the nanoscale makes it possible to study important properties on small coatings and particles in materials as they get more advanced. Nanoindentation provides information on elastic limit and yield strength in addition to hardness, elastic modulus, creep, fracture toughness, etc. making it a versatile metrology instrument.
The stress-strain data provided by nanoindentation in this study identifies the elastic limit of the material while only going 1.2 microns into the surface. We use CSM to determine how mechanical properties of materials develop as an indenter travels deeper into the surface. This is especially useful in thin film applications where properties can be depth dependent. Nanoindentation is a minimally invasive method of confirming material properties in test samples.
The CSM test is useful in measuring material properties versus depth. Cyclical tests can be performed at constant loads to determine more complex material properties. This can be useful to study fatigue or eliminate the effect of porosity to obtain true elastic modulus.
Measurement Objective
In this application, the Nanovea mechanical tester uses CSM to study hardness and elastic modulus versus depth and stress-strain data on a standard steel sample. Steel was chosen for its commonly recognized characteristics to display the control and accuracy of the nanoscale stress-strain data. A spherical tip with a 5-micron radius was used to reach high enough stresses beyond the elastic limit for steel.
Test Conditions & Procedures
The following indentation parameters were used:
Results:
Increase in load during oscillations provide the following depth versus load curve. Over 100 oscillations were conducted during loading to find the stress-strain data as the indenter penetrates the material.
We determined stress and strain from the information obtained at each cycle. The maximum load and depth at each cycle allows us to calculate the maximum stress applied in each cycle to the material. Strain is calculated from the residual depth at each cycle from the partial unloading. This allows us to calculate the radius of the residual imprint by dividing the radius of the tip to give the strain factor. Plotting stress versus strain for the material shows the elastic and plastic zones with the corresponding elastic limit stress. Our tests determined the transition between the elastic and plastic zones of the material to be around 0.076 strain with an elastic limit of 1.45 GPa.
Each cycle acts as a single indent so as we increase load, we run tests at various controlled depths in the steel. So, hardness and elastic modulus versus depth can be plotted directly from the data obtained for each cycle.
As the indenter travels into the material we see hardness increase and elastic modulus decrease.
Conclusion
We have shown the Nanovea mechanical tester provides reliable stress-strain data. Using a spherical tip with CSM indentation allows for material property measurement under increased stress. Load and indenter radius can be changed to test various materials at controlled depths. Nanovea mechanical testers provide these indentation tests from the sub mN range to 400N.
Grooved Stent Coating Failure Using Nano Scratch Testing
Drug–eluting stent is a novel approach in stent technology. It possesses a biodegradable and biocompatible polymer coating that releases medicine slowly and continuously at the local artery to inhibit intimal thickening and prevent the artery from being blocked again. One of the major concerns is the delamination of the polymer coating that carries the drug-eluting layer from the metal stent substrate. In order to improve the adhesion of this coating to the substrate, the stent is designed in different shapes. Specifically in this study, the polymer coating locates at the bottom of the groove on the mesh wire, which brings enormous challenge to the adhesion measurement. A reliable technique is in need to quantitatively measure the interfacial strength between the polymer coating and the metal substrate. The special shape and the small diameter of the stent mesh (comparable to a human hair) require ultrafine X-Y lateral accuracy to locate the test position and proper control and measurement of the load and depth during the test.
Brush Bristle Stiffness Performance Using Tribometer
Brushes are among the most basic and widely used tools in the world. They can be used to remove material (toothbrush, archaeological brush, bench grinder brush), apply material (paintbrush, makeup brush, gilding brush), comb filaments, or add a pattern. As a result of the mechanical and abrasive forces on them, brushes constantly have to be replaced after moderate use. For example toothbrush heads should be replaced every three to four months because of fraying as a result of repeated usage. Making the toothbrush fiber filaments too stiff risks wearing away the actual tooth instead of soft plaque. Making the toothbrush fibers too soft makes the brush lose its form faster. Understanding the changing bend of the brush, as well as the wear and overall change in shape in the filaments under different loading conditions is necessary to design brushes that better fulfill their application.
Low Temperature Tribology
A reliable measurement of low temperature tribology, static and dynamic coefficient of friction, COF, as well as wear behavior is needed in order to better understand the tribological performance of materials for sub-zero applications. It provides a useful tool to correlate the frictional property with the influence of various factors, such as reactions at the interface, interlocking surface features, cohesion of surface films, and even microscopic solid static junctions between surfaces at low temperatures.
Macro Adhesion Failure of DLC
bits and bearings. Under such extreme conditions, sufficient cohesive and adhesive strength of the coating/substrate system becomes vital. In order to select the best metal substrate for the target application and to establish a consistent coating process for DLC, it is critical to develop a reliable technique to quantitatively assess cohesion and adhesion failure of different DLC coating systems.
Cohesive & Adhesive Strength of DLC Using Macro Scratch Testing
High Temperature Scratch Hardness Using Tribometer
Materials are selected based on the service requirements. For applications involving significant temperature changes and thermal gradients, it is critical to investigate the mechanical properties of materials at high temperatures to be fully aware of the mechanical limits. Materials, especially polymers, usually soften at high temperatures. A lot of mechanical failures are caused by creep deformation and thermal fatigue taking place only at elevated temperatures. Therefore, a reliable technique for measuring high temperature scratch hardness is in need to ensure proper selection of the materials for high temperature applications.
High Temperature Scratch Hardness Using Tribometer
Scratch Hardness Measurement Using Tribometer
In this study, the Nanovea Tribometer is used to measure the scratch hardness of different metals. The
capacity of performing scratch hardness measurement with high precision and reproducibility makes
Nanovea Tribometer a more complete system for tribological and mechanical evaluations.
Mechanical & Tribological Properties of Carbon Fiber
Combined with the wear test by Tribometer and surface analysis by Optical 3D Profilometer, we
showcase the versatility and accuracy of the Nanovea instruments in testing composite materials
with directional mechanical properties.
