Tribology testing · Scratch module

Scratch Testing on a Tribometer

In a scratch test, a diamond or tungsten carbide stylus is drawn across a surface under a constant or steadily increasing load. Progressive-load scratches find the critical loads at which a coating cracks, chips or delaminates; constant-load scratches give scratch hardness. On a NANOVEA tribometer the scratch runs on the same platform as friction and wear tests, at macro-scale loads.

At a glance

Modes
Progressive-load scratch for adhesion and cohesion failure; constant-load scratch for scratch hardness and surface-uniformity mapping.
Styli
Conico-spherical diamond tips with 200, 500 or 800 µm radius, and WC tips; custom indenters on request.
Failure detection
Critical loads from optical inspection of the scratch, confirmed by the friction, depth and acoustic-emission signals.
Imaging
On the T2000, a camera images the full length of the scratch so failures can be located and re-examined after the test.
Scratch length & rate
Scratches up to 40 mm (T200) or 50 mm (T2000) long, at 0.002 to 10 mm/s, with loading rates of 0.2–100 N/min (T200) or 1–200 N/min (T2000).
Deformation
Depth measurement separates the elastic and plastic parts of the deformation.
Environments
Heated liquid to 150 °C, humidity, cooling to -40 °C, corrosive media, inert gas; high-temperature scratch hardness in the oven.

What a scratch test tells you

Coatings fail in characteristic ways when a hard stylus is dragged across them under increasing load: tensile cracks behind the stylus, chipping at the edges, buckling, then full delamination. The load at which each failure first appears is a critical load, a practical measure of coating adhesion and cohesion. Critical loads are used to compare coating processes, check production quality and screen substrate preparation.

A constant-load scratch answers a different question: how much the material resists plastic deformation. That is its scratch hardness, calculated from the scratch width.

How the test works

  1. The sample is fixed on the stage and the stylus (diamond or WC, sphero-conical or Rockwell geometry) is brought into contact.
  2. The stage moves the sample under the stylus while the load is held constant or increased linearly from a start load to an end load.
  3. Friction force, penetration depth and acoustic emission are recorded along the scratch.
  4. The scratch is inspected optically to locate each failure and convert its position to a critical load. On the T2000, video zoom imaging records the full scratch so it can be reviewed later alongside the data.

Reading the signals

Optical inspection is the reference for identifying failures, but the in-situ signals add confidence:

  • Friction often steps up when the stylus breaks through a coating into a softer or rougher substrate.
  • Penetration depth separates elastic from plastic deformation and shows sudden changes at failure.
  • Acoustic emission picks up cracking events, sometimes before damage is visible on the surface.

Correlating all three with the scratch image makes the reported critical loads defensible, especially for brittle and transparent coatings.

Progressive versus constant load

Progressive load is the standard approach for adhesion (ASTM C1624, ISO 20502, EN 1071-3, ASTM D7027): a single scratch spans the full load range and reveals every failure stage in sequence. It needs active load control, so it runs on the pneumatic T200 and T2000.

Constant load is used for scratch hardness (ASTM G171) and for mapping: repeating scratches at one load across a surface checks uniformity. Constant-load scratches are also possible on the dead-weight T50.

Tribometer scratch versus micro and nano scratch

The tribometer scratch module covers macro-scale loads, suited to thick, hard coatings and paints, and to polymers and bulk materials. For thin films, NANOVEA’s mechanical testers run micro and nano scratch tests with lower loads and finer load resolution; see adhesive failure and cohesive failure testing. Choosing the platform by load range keeps the critical loads well within the resolved range of the instrument.

Standards

StandardScope
ASTM C1624Adhesion strength and mechanical failure modes of ceramic coatings by quantitative single point scratch testing

Progressive-load scratch with optical identification of critical loads for hard coatings.

ISO 20502Fine ceramics: determination of adhesion of ceramic coatings by scratch testing

Progressive-load scratch adhesion of ceramic coatings.

EN 1071-3Ceramic coatings: determination of adhesion and other mechanical failure modes by a scratch test

Critical loads for cohesive and adhesive failure of thin ceramic coatings.

ASTM D7027Scratch resistance of polymeric coatings and plastics using an instrumented scratch machine

Progressive-load scratches on plastics and polymer coatings, with damage onset correlated to load.

ISO 1518Paints and varnishes: determination of scratch resistance

Constant-load and variable-load scratch resistance of paint films.

ASTM G171Scratch hardness of materials using a diamond stylus

Constant-load scratch; scratch hardness is calculated from the residual scratch width. Also run at elevated temperature.

Instrument parameter limits may differ from those specified within each standard. Ask us which parameters a given configuration covers.

Test environments

Instruments that run this test

Every instrument is built to order. Send us your samples and we run your test in our laboratory first, then configure the instrument around the result.

Published results

Measured in our own laboratory, on the instruments we design and build, and published with full test parameters.

All tribology application notes →

Independent published research

NANOVEA instruments appear in 555 published studies on friction and wear, by researchers at universities and industrial laboratories worldwide.

All 555 studies →

NANOVEA materials testing laboratory

Send us your coated samples.

Our laboratory runs scratch adhesion and scratch hardness tests from nano to macro loads, on tribometers and mechanical testers, and reports critical loads with images of each failure.

Your samples are tested by the people who design the instruments, so you get advice on the method as well as the numbers.

Indentation & scratch lab services

Frequently asked questions

What does a scratch test measure?

A progressive-load scratch test measures the critical loads at which a coating fails: first cohesive failures such as cracking within the coating, then adhesive failure where it separates from the substrate. A constant-load scratch measures scratch hardness, the resistance to plastic deformation, from the width of the residual scratch.

How are critical loads identified?

Primarily by optical inspection of the scratch, locating each failure and converting its position to the load applied at that point. The friction force, penetration depth and acoustic-emission signals recorded during the scratch help confirm where failures start, which is especially useful for brittle coatings.

When should I scratch test on a tribometer rather than a mechanical tester?

Use a tribometer for macro-scale loads: thick or very hard coatings, paints and polymers that need higher forces, and when you also want friction and wear data from the same platform. Use a NANOVEA mechanical tester for micro and nano scratch on thin films, where lower loads and finer load resolution are needed.

How is scratch hardness calculated?

ASTM G171 calculates scratch hardness from the applied normal load and the width of the residual scratch made by a diamond stylus of defined geometry. A harder material leaves a narrower scratch at the same load. Widths can be measured optically or with a 3D profilometer.

Can scratch tests be run at high temperature?

Yes. Constant-load scratch hardness can be measured inside the tribometer's oven. NANOVEA's published study measured Teflon from room temperature to 300 °C, showing the scratch width nearly doubling as the polymer softened.

Which tribometers support scratch testing?

Progressive-load scratch adhesion testing runs on the pneumatic T200 and T2000, which can ramp the load during the scratch. Constant-load scratch hardness is also possible on the dead-weight T50.