Tribology testing · Humidity & inert gas module

Humidity & Inert Gas Tribology Testing

The humidity and inert gas module encloses the tribological contact so its atmosphere can be controlled: relative humidity from 10% to 90%, or a purge with inert gas. Water vapour and oxygen change friction and wear in many materials, sometimes by an order of magnitude, so environment-sensitive coatings must be tested in a known atmosphere.

Humidity and inert gas enclosure on a NANOVEA T50 tribometer

At a glance

Humidity range
Relative humidity controlled from 10% to 90%.
Control
A humidity controller attached to the chamber holds the set relative humidity to within ±1%.
Inert gas
The same enclosure can be purged with inert gas to exclude oxygen and moisture.
Modules
Rotational, linear and scratch; block-on-ring and ring-on-ring as custom configurations.
Measurements
Friction and wear as a function of relative humidity or atmosphere; wear rate from 3D profilometry.
Typical materials
DLC and other carbon coatings, solid lubricants, glass and its coatings, polymers, hygroscopic materials.

Why the atmosphere matters

Friction and wear are not intrinsic material properties. They belong to the whole tribosystem, and the surrounding gas is part of that system. Water vapour adsorbs on surfaces within seconds, oxygen drives oxidation and tribochemical films, and both are present in room air in amounts that vary with season, weather and laboratory. A coating qualified on a dry winter day can behave differently on a humid summer one.

Controlling the atmosphere makes results repeatable from day to day and lab to lab, and it lets the effect of humidity be measured deliberately rather than suffered as noise.

How the module works

The contact is enclosed in a chamber connected to a humidity controller, which sets relative humidity anywhere from 10% to 90% and holds it to within ±1%. The same enclosure can instead be fed with inert gas to purge oxygen and moisture. Rotational, linear and scratch tests run inside it as normal; block-on-ring and ring-on-ring can be enclosed as custom configurations.

A typical study runs the same test at several humidity set points (for example 10%, 30% and 60% RH) and compares friction curves, wear rates and wear morphology.

DLC: a material defined by its environment

Diamond-like carbon is the classic environment-sensitive coating. In NANOVEA’s DLC humidity study against a silicon nitride ball:

  • at 10% RH, COF stayed around 0.05 throughout the test;
  • at 30% RH, COF settled around 0.1;
  • above 50% RH, a distinct run-in stage appeared over the first 2000 revolutions.

The ball’s wear scar was smaller at low humidity. In dry conditions a stable DLC transfer layer built up on the ball, so the coating slid against its own transfer film, which acted as an efficient solid lubricant.

Coatings that must survive the weather

Exterior coatings meet a wide humidity range in service. NANOVEA tested self-cleaning glass coatings at 30% and 60% RH against a WC ball. At 30% RH, uncoated glass started at COF ~0.45 and climbed to ~0.6, while both coatings started below 0.2; one stayed near 0.25 and the other rose sharply partway through the test. Testing at more than one humidity revealed differences in durability that a single room-air test would not.

Measuring the wear

After the test, the wear track is measured by chromatic confocal 3D non-contact profilometry. It handles transparent and highly reflective surfaces such as glass and DLC, and gives the worn volume for the specific wear rate K = V / (F × s) at each humidity.

Tests you can run in a controlled atmosphere

Instruments that run this test

Every instrument is built to order. Send us your samples and we run your test in our laboratory first, then configure the instrument around the result.

Published results

Measured in our own laboratory, on the instruments we design and build, and published with full test parameters.

All tribology application notes →

Independent published research

NANOVEA instruments appear in 555 published studies on friction and wear, by researchers at universities and industrial laboratories worldwide.

All 555 studies →

NANOVEA materials testing laboratory

Environment-sensitive coating? Send us your samples.

Our laboratory runs friction and wear tests at controlled humidity and in inert gas on the same instruments we build, and reports results with the full test parameters and atmosphere.

Your samples are tested by the people who design the instruments, so you get advice on the method as well as the numbers.

Friction & wear lab services

Frequently asked questions

Why does humidity affect friction and wear?

Adsorbed water changes the chemistry and mechanics of the contact. It can passivate or lubricate surfaces, alter how transfer layers form, promote tribochemical reactions, or soften hygroscopic materials. The effect depends on the material: some coatings perform best dry and others need moisture, so a single room-air test can be misleading.

Why is DLC sensitive to humidity?

In dry conditions, many DLC coatings form a stable graphitic transfer layer on the counterface and then slide against their own transfer film, which gives very low friction and wear. Moisture interferes with that layer. NANOVEA's published study measured COF ~0.05 at 10% RH and ~0.1 at 30% RH, with a longer run-in at higher humidity.

What humidity range can be controlled?

Relative humidity from 10% to 90%, with the set point held to within ±1% by the controller attached to the chamber. Inert gas can be fed through the same enclosure for dry, oxygen-free tests.

Can tribology tests run in vacuum?

Yes, as a custom configuration. NANOVEA vacuum systems start at 10⁻⁵ Torr and can be combined with humidity, inert gas and high temperature, for friction, wear and scratch tests on materials meant for space or other vacuum service.

Why test in inert gas?

Purging with inert gas removes oxygen and moisture from the contact. That separates mechanical wear from oxidation and tribochemistry, simulates sealed or protective-atmosphere service, and approximates dry, oxygen-free conditions for materials intended for space or vacuum use.

Which tests run under controlled humidity?

Rotational (pin-on-disk), linear reciprocating and scratch tests, with block-on-ring and ring-on-ring available as custom configurations.