Mechanical testing · Liquid module

Nanoindentation, Scratch & Friction in Liquid

The liquid module holds the sample immersed during nanoindentation, scratch and friction tests, in water, saline, simulated body fluid, lubricant or any service liquid. The liquid can be heated from room temperature up to 60 °C, which covers physiological temperature. Hydrated materials such as hydrogels, tissues and many polymers must be tested wet, because drying changes their properties.

Liquid cell for testing immersed samples on a NANOVEA mechanical tester

At a glance

Configuration
Liquid cup holding the sample immersed during the test, with custom cup designs to suit the sample and application.
Heating
Liquid temperature from room temperature up to 60 °C, on both the nano and micro modules.
Tests
Nanoindentation hardness, modulus and creep; nano and micro scratch; low-load friction.
Liquids
Water, saline and simulated body fluids (e.g. Hanks' solution), lubricants and process liquids.
Materials
Hydrogels, tissues, biomaterials, medical device coatings, polymers and coatings in service fluids.
Platforms
PB1000 and CB500 mechanical testers.

Why test in liquid

Hydrogels, cartilage, tissues and many polymers are defined by their water content; measured dry, they are effectively different materials. Medical devices, implants and their coatings work immersed in body fluids, and many industrial coatings and seals work in liquids. Testing in the liquid keeps the material in its real state and the contact in its real environment.

How the module works

The sample sits in a liquid cup, designed to suit the sample, and stays immersed throughout the test. The indenter or stylus works through the liquid. The liquid can be heated from room temperature up to 60 °C. The same nanoindentation, scratch and friction tests run as in air, with the liquid changing only the environment, not the method.

Testing soft, hydrated materials

Very soft hydrated materials need adapted test conditions. In NANOVEA’s hydrogel study, a 3 mm spherical tip at 10 mN measured ~42 µm of creep in 70 s, and the initial contact was complicated by surface tension pulling the ball into the gel before load registered. Large tips, low loads and careful contact analysis make such measurements reliable.

Medical devices and biomaterials

Device materials are best compared in the fluid they will meet. NANOVEA compared silicone and polyether-polyurethane pacing-lead insulation in Hanks’ solution: low-load friction at 50 mN, then wear, with the silicone showing a wear scar about twice as wide (~1.2 mm vs ~0.6 mm).

Tests you can run in liquid

Instruments that run this test

Every instrument is built to order. Send us your samples and we run your test in our laboratory first, then configure the instrument around the result.

Published results

Measured in our own laboratory, on the instruments we design and build, and published with full test parameters.

All mechanical testing application notes →

Independent published research

NANOVEA instruments appear in 438 published studies on indentation, hardness and scratch, by researchers at universities and industrial laboratories worldwide.

All 438 studies →

NANOVEA materials testing laboratory

Hydrated or medical samples? Send them to us.

Our laboratory runs nanoindentation, scratch and friction tests on immersed samples on the same mechanical testers we build, and reports results with the full test parameters and liquid conditions.

Your samples are tested by the people who design the instruments, so you get advice on the method as well as the numbers.

Indentation & scratch lab services

Frequently asked questions

Why test samples immersed in liquid?

Hydrated materials change when they dry: hydrogels shrink and stiffen, tissues and many polymers become harder, and surface properties change. Testing immersed keeps the material in its service state. Immersion also lets coatings and devices be tested in the fluid they will meet, such as simulated body fluid for implants.

What liquids can be used?

Water, saline and simulated body fluids such as Hanks' solution, lubricants and other process liquids, chosen to match the application.

Can the liquid be heated?

Yes, from room temperature up to 60 °C, so tests can run at body temperature (37 °C) or at warm service conditions. For liquid tests at higher temperatures under tribological loads, NANOVEA tribometers heat liquids up to 150 °C.

What is special about indenting soft hydrated materials?

Contact detection is difficult because the surface offers almost no resistance, and liquid surface tension can pull the tip in before any load registers. Large spherical tips, low loads and careful analysis of the approach are used. NANOVEA's hydrogel study used a 3 mm sphere at 10 mN and observed exactly this surface-tension effect.

Can medical device coatings be tested in liquid?

Yes. Friction and scratch tests of coatings and polymers can run immersed in simulated body fluid. NANOVEA has compared the friction of pacing-lead insulation materials immersed in Hanks' solution.