{"id":10671,"date":"2021-03-03T18:41:38","date_gmt":"2021-03-03T18:41:38","guid":{"rendered":"https:\/\/nanovea.com\/?p=10671"},"modified":"2025-05-22T20:46:52","modified_gmt":"2025-05-22T20:46:52","slug":"metalurji%cc%87-cok-fazli-malzeme-calismasi","status":"publish","type":"post","link":"https:\/\/nanovea.com\/tr\/metallurgy-study-of-multiphase-material\/","title":{"rendered":"\u00c7ok Fazl\u0131 Metal Nanoindentasyon"},"content":{"rendered":"
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Nanoindentasyon Kullan\u0131larak \u00c7ok Fazl\u0131 Malzemelerin Metalurji \u00c7al\u0131\u015fmas\u0131<\/p>

Daha fazla bilgi edinin<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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METALURJI\u0307 \u00c7ALI\u015eMASI
\u00c7OK FAZLI MALZEMENIN<\/span><\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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NANOINDENTASYON KULLANARAK<\/span><\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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Taraf\u0131ndan haz\u0131rlanm\u0131\u015ft\u0131r<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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DUANJIE LI<\/span>, Doktora <\/span>& <\/span>ALEXIS CELESTIN<\/span><\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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G\u0130R\u0130\u015e<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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Metalurji, metalik elementlerin yan\u0131 s\u0131ra bunlar\u0131n metaller aras\u0131 bile\u015fikleri ve ala\u015f\u0131mlar\u0131n\u0131n fiziksel ve kimyasal davran\u0131\u015flar\u0131n\u0131 inceler. D\u00f6k\u00fcm, d\u00f6vme, haddeleme, ekstr\u00fczyon ve i\u015fleme gibi i\u015flemlerden ge\u00e7en metaller fazlar\u0131nda, mikro yap\u0131lar\u0131nda ve dokular\u0131nda de\u011fi\u015fiklikler ya\u015farlar. Bu de\u011fi\u015fiklikler, malzemenin sertlik, mukavemet, tokluk, s\u00fcneklik ve a\u015f\u0131nma direnci gibi \u00e7e\u015fitli fiziksel \u00f6zellikleriyle sonu\u00e7lan\u0131r. Metalografi genellikle bu t\u00fcr spesifik fazlar\u0131n, mikroyap\u0131n\u0131n ve dokunun olu\u015fum mekanizmas\u0131n\u0131 \u00f6\u011frenmek i\u00e7in uygulan\u0131r.<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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YEREL MEKANI\u011eIN \u00d6NEMI\nMALZEME TASARIMI I\u00c7IN \u00d6ZELLIKLER<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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Geli\u015fmi\u015f malzemeler, end\u00fcstriyel uygulamalarda hedeflenen mekanik \u00f6zellikleri elde etmek i\u00e7in genellikle \u00f6zel bir mikroyap\u0131 ve dokuda birden fazla faza sahiptir. Nanoindentasyon<\/a> malzemelerin mekanik davran\u0131\u015flar\u0131n\u0131 k\u00fc\u00e7\u00fck \u00f6l\u00e7eklerde \u00f6l\u00e7mek i\u00e7in yayg\u0131n olarak uygulanmaktad\u0131r i ii<\/sup>.\u00a0<\/sup>Bununla birlikte, \u00e7ok k\u00fc\u00e7\u00fck bir alanda girinti i\u00e7in belirli konumlar\u0131 hassas bir \u015fekilde se\u00e7mek zor ve zaman al\u0131c\u0131d\u0131r. Bir malzemenin farkl\u0131 fazlar\u0131n\u0131n mekanik \u00f6zelliklerini y\u00fcksek hassasiyet ve zaman\u0131nda \u00f6l\u00e7\u00fcmlerle belirlemek i\u00e7in g\u00fcvenilir ve kullan\u0131c\u0131 dostu bir nano indentasyon testi prosed\u00fcr\u00fc talep edilmektedir.<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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\u00d6L\u00c7\u00dcM HEDEFI<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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Bu uygulamada, En G\u00fc\u00e7l\u00fc Mekanik Test Cihaz\u0131 olan NANOVEA PB1000'i kullanarak \u00e7ok fazl\u0131 bir metal\u00fcrjik numunenin mekanik \u00f6zelliklerini \u00f6l\u00e7\u00fcyoruz.<\/em><\/p>

Burada, Geli\u015fmi\u015f Pozisyon Kontrol\u00f6r\u00fcm\u00fcz\u00fc kullanarak PB1000'in b\u00fcy\u00fck bir numune y\u00fczeyinin birden fazla faz\u0131nda (tanecik) nanoindentasyon \u00f6l\u00e7\u00fcmlerini y\u00fcksek hassasiyet ve kullan\u0131c\u0131 dostu bir \u015fekilde ger\u00e7ekle\u015ftirme kapasitesini sergiliyoruz.<\/em><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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NANOVEA<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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PB1000<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t

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\n\t\t\t\t\t\t\t\t\tTEST KO\u015eULLARI\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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Bu \u00e7al\u0131\u015fmada, \u00e7ok fazl\u0131 bir metal\u00fcrjik numune kulland\u0131k. Numune, girinti testlerinden \u00f6nce ayna benzeri bir y\u00fczey fini\u015fine kadar parlat\u0131lm\u0131\u015ft\u0131r. Numunede a\u015fa\u011f\u0131da g\u00f6sterildi\u011fi gibi FAZ 1, FAZ 2, FAZ 3 ve FAZ 4 olmak \u00fczere d\u00f6rt faz tespit edilmi\u015ftir.<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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Geli\u015fmi\u015f Sahne Kontrol\u00f6r\u00fc, farenin konumuna ba\u011fl\u0131 olarak optik mikroskop alt\u0131nda numune hareketinin h\u0131z\u0131n\u0131 otomatik olarak ayarlayan sezgisel bir numune gezinme arac\u0131d\u0131r. Fare g\u00f6r\u00fc\u015f alan\u0131n\u0131n merkezinden ne kadar uzakta olursa, sahne farenin y\u00f6n\u00fcne do\u011fru o kadar h\u0131zl\u0131 hareket eder. Bu, t\u00fcm numune y\u00fczeyinde gezinmek ve mekanik test i\u00e7in istenen konumu se\u00e7mek i\u00e7in kullan\u0131c\u0131 dostu bir y\u00f6ntem sa\u011flar. Test konumlar\u0131n\u0131n koordinatlar\u0131, y\u00fckler, y\u00fckleme\/bo\u015faltma h\u0131z\u0131, bir haritadaki test say\u0131s\u0131 vb. gibi bireysel test kurulumlar\u0131yla birlikte kaydedilir ve numaraland\u0131r\u0131l\u0131r. Bu t\u00fcr bir test prosed\u00fcr\u00fc, kullan\u0131c\u0131lar\u0131n geni\u015f bir numune y\u00fczeyini indentasyon i\u00e7in belirli ilgi alanlar\u0131 a\u00e7\u0131s\u0131ndan incelemesine ve t\u00fcm indentasyon testlerini farkl\u0131 konumlarda tek seferde ger\u00e7ekle\u015ftirmesine olanak tan\u0131yarak \u00e7ok fazl\u0131 metalurjik numunelerin mekanik testleri i\u00e7in ideal bir ara\u00e7 haline getirir.<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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Bu \u00e7al\u0131\u015fmada, optik mikroskop alt\u0131nda numunenin spesifik fazlar\u0131n\u0131 <\/span>NANOVEA <\/span>Mekanik Test Cihaz\u0131 \u00fczerinde numaraland\u0131r\u0131ld\u0131\u011f\u0131 gibi <\/span>\u015eEK\u0130L 1<\/span>. Se\u00e7ilen konumlar\u0131n koordinatlar\u0131 kaydedilir ve ard\u0131ndan a\u015fa\u011f\u0131da \u00f6zetlenen test ko\u015fullar\u0131 alt\u0131nda tek seferde otomatik nanoindentasyon testleri ger\u00e7ekle\u015ftirilir<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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\n\t\t\t\t\t\t\t\t\t\u015eEK\u0130L 1: <\/span>NUMUNE Y\u00dcZEYINDE NANOINDENTASYON KONUMUNUN SE\u00c7ILMESI.<\/span>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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\n\t\t\t\t\t\t\t\t\tSONU\u00c7LAR: <\/span>FARKLI FAZLAR \u00dcZERINDE NANOINDENTASYONLAR<\/span>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t
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Numunenin farkl\u0131 a\u015famalar\u0131ndaki girintiler a\u015fa\u011f\u0131da g\u00f6sterilmi\u015ftir. Numune a\u015famas\u0131n\u0131n m\u00fckemmel pozisyon kontrol\u00fcn\u00fcn <\/span>NANOVEA <\/span>Mekanik Test Cihaz\u0131<\/a> kullan\u0131c\u0131lar\u0131n mekanik \u00f6zellik testleri i\u00e7in hedef konumu tam olarak belirlemelerine olanak tan\u0131r.<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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\u00c7entiklerin temsili y\u00fck-deplasman e\u011frileri a\u015fa\u011f\u0131da g\u00f6sterilmi\u015ftir <\/span>\u015eEK\u0130L 2<\/span>ve Oliver ve Pharr Y\u00f6ntemi kullan\u0131larak hesaplanan kar\u015f\u0131l\u0131k gelen sertlik ve Young's Mod\u00fcl\u00fciii<\/sup><\/span> <\/span>'de \u00f6zetlenmi\u015f ve kar\u015f\u0131la\u015ft\u0131r\u0131lm\u0131\u015ft\u0131r. <\/span>\u015eEK\u0130L 3<\/span>.<\/span><\/p>\n


Bu <\/span>1., 2., 3. A\u015eAMALAR <\/span>ve <\/span>4 <\/span>s\u0131ras\u0131yla ~5.4, 19.6, 16.2 ve 7.2 GPa ortalama sertli\u011fe sahiptir. Nispeten k\u00fc\u00e7\u00fck boyut i\u00e7in <\/span>2. A\u015eAMA <\/span>sertlik ve Young's Mod\u00fcl\u00fc de\u011ferlerinin daha y\u00fcksek standart sapmas\u0131na katk\u0131da bulunur.<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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\n\t\t\t\t\t\t\t\t\t\u015eEK\u0130L 2: <\/span>Y\u00dcK-DEPLASMAN E\u011eRILERI <\/br>\nNANOINDENTASYONLARIN<\/span>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t
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\u015eEK\u0130L 3: <\/span>FARKLI FAZLARIN SERTLIK VE YOUNG MOD\u00dcL\u00dc<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t

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SONU\u00c7<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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Bu \u00e7al\u0131\u015fmada, Geli\u015fmi\u015f A\u015fama Kontrol\u00f6r\u00fcn\u00fc kullanarak b\u00fcy\u00fck bir metal\u00fcrjik numunenin birden fazla faz\u0131 \u00fczerinde nanoindentasyon \u00f6l\u00e7\u00fcmleri yapan NANOVEA Mekanik Test Cihaz\u0131n\u0131 sergiledik. Hassas konum kontrol\u00fc, kullan\u0131c\u0131lar\u0131n b\u00fcy\u00fck bir numune y\u00fczeyinde kolayca gezinmesine ve nanoindentasyon \u00f6l\u00e7\u00fcmleri i\u00e7in ilgilenilen alanlar\u0131 do\u011frudan se\u00e7mesine olanak tan\u0131r.<\/p>

T\u00fcm girintilerin konum koordinatlar\u0131 kaydedilir ve ard\u0131ndan ard\u0131\u015f\u0131k olarak ger\u00e7ekle\u015ftirilir. B\u00f6yle bir test prosed\u00fcr\u00fc, bu \u00e7al\u0131\u015fmadaki \u00e7ok fazl\u0131 metal numune gibi k\u00fc\u00e7\u00fck \u00f6l\u00e7eklerde yerel mekanik \u00f6zelliklerin \u00f6l\u00e7\u00fcm\u00fcn\u00fc \u00f6nemli \u00f6l\u00e7\u00fcde daha az zaman al\u0131c\u0131 ve daha kullan\u0131c\u0131 dostu hale getirmektedir. Sert FAZ 2, 3 ve 4, FAZ 1 i\u00e7in ~5,4 GPa'ya k\u0131yasla s\u0131ras\u0131yla ~19,6, 16,2 ve 7,2 GPa ortalama sertli\u011fe sahip olarak numunenin mekanik \u00f6zelliklerini iyile\u015ftirmektedir.<\/p>

Cihaz\u0131n Nano, Mikro veya Makro mod\u00fcllerinin t\u00fcm\u00fc ISO ve ASTM uyumlu girinti, \u00e7izik ve a\u015f\u0131nma test modlar\u0131n\u0131 i\u00e7erir ve tek bir sistemde mevcut olan en geni\u015f ve en kullan\u0131c\u0131 dostu test yelpazesini sa\u011flar. NANOVEA'n\u0131n e\u015fsiz \u00fcr\u00fcn yelpazesi, sertlik, Young mod\u00fcl\u00fc, k\u0131r\u0131lma toklu\u011fu, yap\u0131\u015fma, a\u015f\u0131nma direnci ve di\u011ferleri dahil olmak \u00fczere ince veya kal\u0131n, yumu\u015fak veya sert kaplamalar\u0131n, filmlerin ve alt tabakalar\u0131n t\u00fcm mekanik \u00f6zelliklerini belirlemek i\u00e7in ideal bir \u00e7\u00f6z\u00fcmd\u00fcr.<\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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i <\/span>Oliver, W. C.; Pharr, G. M., Malzeme Ara\u015ft\u0131rmalar\u0131 Dergisi, Cilt 19, Say\u0131 1, Ocak 2004, s.3-20
<\/span>ii <\/span>Schuh, C.A., Materials Today, Cilt 9, Say\u0131 5, May\u0131s 2006, s. 32-40
<\/span>iii <\/span>Oliver, W. C.; Pharr, G. M., Malzeme Ara\u015ft\u0131rmalar\u0131 Dergisi, Cilt 7, Say\u0131 6, Haziran 1992, s.1564-1583<\/span><\/p>\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t

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Benzer bir uygulaman\u0131z var m\u0131?<\/h2>\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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\n\t\t\t\t\t\n\t\t\t\t\t\t\n\t\t\t\t\t\t\t\t\t\u015eIMDI BIR UZMANLA G\u00d6R\u00dc\u015e\u00dcN<\/span>\n\t\t\t\t\t<\/span>\n\t\t\t\t\t<\/a>\n\t\t\t\t<\/div>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t
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\n\t\t\t\t\t\n\t\t\t\t\t\t\n\t\t\t\t\t\t\t\t\tFI\u0307YATLANDIRMA VE DETAYLARI HIZLI ALIN<\/span>\n\t\t\t\t\t<\/span>\n\t\t\t\t\t<\/a>\n\t\t\t\t<\/div>\n\t\t\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t<\/div>","protected":false},"excerpt":{"rendered":"

Nanoindentasyon Kullan\u0131larak \u00c7ok Fazl\u0131 Malzemelerin Metalurji \u00c7al\u0131\u015fmas\u0131 Daha fazla bilgi edinin<\/p>","protected":false},"author":1,"featured_media":10763,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_exactmetrics_skip_tracking":false,"_exactmetrics_sitenote_active":false,"_exactmetrics_sitenote_note":"","_exactmetrics_sitenote_category":0,"footnotes":""},"categories":[7,338,349,337],"tags":[],"class_list":["post-10671","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-application-notes","category-indentation-hardness-elastic","category-laboratory-testing","category-mechanical-testing"],"_links":{"self":[{"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/posts\/10671","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/comments?post=10671"}],"version-history":[{"count":66,"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/posts\/10671\/revisions"}],"predecessor-version":[{"id":24749,"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/posts\/10671\/revisions\/24749"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/media\/10763"}],"wp:attachment":[{"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/media?parent=10671"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/categories?post=10671"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/nanovea.com\/tr\/wp-json\/wp\/v2\/tags?post=10671"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}